Sea water sample measurement and small sample volume options have also. Examining the role of toc analyzers in the pharmaceutical laboratory. Toccontrol l software combines new features with easytouse operation. In the first tab parameters sample name, manual dilution ratio, sample id and number of determinations can be changed. Open the tocl sample table editor by double clicking the shortcut on the desktop. Operation guide for lcmssolution pdf version cdrom disk for installation provides the operation guide volume of the instruction manual as a pdf file so that it can be viewed on your personal computer. Instrument blue text marks the name of the window to which the text refers. Consisting of four models, including pccontrolled and standalone versions, the tocl uses shimadzus 680 c combustion catalytic oxidation method to efficiently analyze all organic compounds.
The sievers 900 series toc analyzers represent the next generation of the bestselling sievers model 800. Enter the serial number of the tocinstrument mentioned on the instrument label. Principle and calibration of toc total organic carbon. Reliable online monitoring of industrial wastewater. Equipment shimadzu hightemperature tocl combustion analyzer. Nonpurgeable organic carbon npoc analysis using the. The sample is acidified and the inorganic carbon is eliminated stripping. Consult shimadzu europas entire tocl catalogue on directindustry. With the tocl series, numerous options enable a variety of functional enhancements. Relevant instruction manuals name content tocv user manual describes the procedures necessary for performing. It is utilized to determine the carbonnitrogen content in fluids and sludge. Virtual advisor shimadzu has launched its interactive virtual advisor website to further enhance customer service. Used shimadzu tocl csn total organic carbon analyzer lab.
Once the sample is in place, close the chamber and click ok. User id user name the user id is entered for use in login, and the user name is entered to associate the user id with a proper name. The tocl series provides even better functionality and operability than the popular tocv series. This system is an exceptional offering, with all required software, manual, and autosampler option.
Table of contents table of content toccontrol v main menu 1. Find sample dilution equipment related suppliers, manufacturers, products and specifications on globalspec a trusted source of sample dilution equipment information. The software does not permit multiple use of identical user ids or user names. One of its most important features is the capacity to efficiently oxidize hardtodecompose organic compounds, including insoluble and macromolecular organic compounds. To change the other settings, rightclick on the row that you would like and select measurement settings. C391e084 tocl series shimadzu total organic carbon. After a short registration step, the user will be offered a host of information relating to hplc, uflc, lcms, toc v and toc l series like flow diagrams, daily and periodic maintenance and troubleshooting. These include simultaneous measurement of toc and tn total nitrogen when a tn unit is added, the use of compressor air when a carrier gas purification kit is added, and the measurement of gas samples and solid samples when a gas sample injection kit and solid sample combustion unit are added. Overview a fully functional toc l can be used for a variety of applications, such as quality control, process control. As the sample moves through the oxidation chamber, it is subjected to highintensity ultraviolet radiation at 185 nm. See the sievers 500 rl and 900 series toc analyzer operation and maintenance manuals. University of maryland center for environmental science. The clear layout of the sample window editor offers users ataglance access to all. Tocl series total organic carbon analyzers from shimadzu description the tocl series of toc analyzers adopts the 680c combustion catalytic oxidation method, which was developed by shimadzu and is now used worldwide.
More pdf, 14 mb information on the applications that can be carried out with this specific device. The total organic carbon analyzer present at the gi facility is a toc l cphcpn analyzer shimadzu. It features automatic sample acidification and sparging, as well as an automatic dilution function that reduces sample salinity, acidity and alkalinity. The shimadzu tocl combustion analyzer is the stateoftheart instrument for analysis of doc and tdn. The available detector sample rates are dependent on the base period settings on the shimadzu lc1020 system setup detector tab by using the shortest base period of 20 ms, the sampling rate can be set up to 50 hz.
Capital program management services public safety portfolio. I used shimadzu tocl liquid analyzer to estimate total organic carbon and total nitrogen for soil samples. Allows for manual entry of different standard solution with one. It measures reliably and accurately even in heavy duty applications with high loads of salt, fat or fibers. B filter sample with a 3 psig nalgene hand vacuum pump and a 47mm whatman gff filter into a burned, amber glass bottle. This instrument provides automated analysis of liquid samples for. This makes the toc l one of the most universal toc analyzers.
Page 1 shimadzu tocv series total organic carbon analyser shortuser manual tocv cphcpn toccontrol v version 2. Rinse bottle twice with tap water and twice with deionized water prior to burning at 500 o c for 4 hours. Developed by shimadzu, the 680c combustion catalytic oxidation method is now used worldwide. The tocl series adopts the 680c combustion catalytic oxidation method, which was developed by shimadzu and is employed with confidence in many reputable oceanographic laboratories around the country. In addition, applications can be further enhanced by adopting new options such as a kit for small sample volumes and a highsalt sample combustion tube kit. Sample analysis is conducted by the shimadzu tocv csh total organic carbon analyzer, using the npoc analysis method. The manual is one of the most informative that i have come across. Shimadzu total organic carbon analyzer labmakelaar.
Offering a dynamic operating range of 50 ppb to 50, 000 ppm. Provides the operation guide volume of the instruction manual as a pdf file so that it can be viewed on your personal computer. The procedures related to toccontrol v software system administration are described in detail in the tocv administrators manual. Ic reagent supply pump phosphoric acid pure water trap back.
Instrumentation and monitoring equipment helps utilities monitor total organic carbon, chlorine, nitrates and other key process variables. Now it is time to place the sample in front of the beam. The procedures related to toc control v software system administration are described in detail in the toc v administrators manual. The tocl series of toc analyzers adopts the 680c combustion catalytic oxidation method, which was developed by shimadzu and is now used worldwide. For example, a blank peak of 1mgl has little influence on results greater than.
Toc application handbook shimadzu scientific instruments. Tocl detection limit high salt catalyst 10mgl range 5. Quality assurance and control protocols are employed throughout sample analysis, including. Consisting of pccontrolled and standalone models, the shimadzu tocl series of laboratory total organic carbon analyzers offers the optimum selection of performance features and options to meet the specific requirements of total organic carbon testing in a wide range of aqueous samples. Beyond analytical performance and compliance, the m9 lab has automated features to save you time, an option for simultaneous stage 1 conductivity testing, and foursecond analysis time in turbo mode. There is a triangular sample holder that can be used. It provides operation and maintenance procedures for the toc v. A free, webbased resource where users can search thousands of applications for use with our analytical and testing instrumentation.
This is the highest level of detection sensitivity available with the combustion. This publication may not be reproduced in whole or in part without the express written permission of. Directions for running ic samples on the shimadzu toc. Being only a 20 model, this is an excellent way to cut costs. It provides operation and maintenance procedures for the tocv. Toc analyzer with priority on easy measurement through manual sample injection and simple operations. Then the sample is transferred through a rotation slit filter in which the particles are separated according to din standards. Tocl laboratory total organic carbon analyzers shimadzu. Relevant instruction manuals name content tocv user. Capital program management services public safety portfolio between cook cotnty government. Basic user guide on creating a calibration curve, manually from an extracted data file, to quantitate unknowns utilizing labsolutions lcgc workstation softw.
This system is an exceptional offering, with all required software, manual, and autosampler. How do you prepare soil samples to measure total organic. The tocl series of toc analyzers adopts the 680c combustion catalytic. It allows you to use each instruction manual via the hyperlink. Total organic carbon analyzer shimadzu scientific instruments. A quality water supply depends on accurate and reliable treatment plant process control. Several power plants prefer to extract a representative sample of fly ash from the process stream, that is tested in a laboratory. Be sure to read this documentation carefully before using the instrument for the first time. The lc2010ht is comprised of a degassing unit, quaternary lowpressure gradient unit, pump unit, mixer, ultra fast autosampler, column oven, and.
Sampling and laboratory analysis treatment plant operator. Ca72toc determines the total organic carbon toc content in a number of industries. If the problem persists, or symptoms not covered in the troubleshooting section occur, contact your shimadzu representative. The instrument is easy to use and the software is user friendly.
The m9 lab offers timetested dependability and accuracy with sievers toc technology. Here are some of the latest sampling and laboratory analysis products offered by industry manufacturers. Further details can be found in the individual application notes for instance. Principle and calibration of toc total organic carbon analyzer. The general table of contents is available, including other instruction manuals pdf versions. Tocl total organic carbon analyzer from shimadzu scientific. This makes the tocl one of the most universal toc analyzers. The tocl series features variable syringe sizes when the sample volume is limited. Sievers innovox toc analyzers are designed to measure organic carbon in a broad range of water samples. Labsolutions lcgc workstation creating a calibration curve. The lc2010ht is a nextgeneration hplc based on the concept of highthroughput analysis and automated validation. Tocl series total organic carbon analyzers from shimadzu. Sop for calibration total organic carbon toc analyzer. Two basic analyzer types can be equipped with many options, kits and numerous accessories and customized to any particular application.
New toc analyzer uses supercritical water oxidation technique environmental. Overview a fully functional tocl can be used for a variety of applications, such as quality control, process control. Toc measurement principle catalytic combustion at 680c 5. Flow line diagrams toclcph highsensitivity model printer acid dilution water asil autosampler electronic gas flowrate controller tc sample injection port, slide type carrier gas multifunction sample pretreatment injection system ultrapure water trap for blank check nondispersive infrared detector ndir ic sample injection port, slide type personal computer not included in the toc. The tocl analyzers to determine toc total organic carbon. Page 5 shimadzu lc1020 system table of contents to facilitate the orientation in the shimadzu lc 1020 system manual and clarity chromatography station, different fonts are used throughout the manual. Soest laboratory for analytical biogeochemistry equipment. View and download shimadzu lc10 user manual online.
The 680 c combustion catalytic oxidation method has been adopted for the tocl series. The most important feature of a toc analyzer is its ability to efficiently oxidize not only easily decomposed, low molecular weight organic compounds, but also hardtodecompose insoluble. Includes tnml total nitrogen measuring unit, asil autosampler, software, manuals, and accessories as pictured skip to navigation skip to content search, browse, and buy used lab. User level selects the user level for the user being registered.
Consisting of pccontrolled and standalone models, the shimadzu toc l series of laboratory total organic carbon analyzers offers the optimum selection of performance features and options to meet the specific requirements of total organic carbon testing in a wide range of aqueous samples. Find toc analyzers maintenance related suppliers, manufacturers, products and specifications on globalspec a trusted source of toc analyzers maintenance information. Nov 08, 2016 basic user guide on creating a calibration curve, manually from an extracted data file, to quantitate unknowns utilizing labsolutions lcgc workstation softw. A virtual advisor tech support site for shimadzus l series line of total organic carbon analyzers. Tape can also be used to hold the sample in front of the beam. A virtual advisor tech support site for shimadzus lseries line of total organic carbon analyzers. Enhancing multianalyte processing when analyzing a large number of analytes, it is crucial to about 14 seconds, the iseries achieves processing speeds reduce the time between analyses, specifically the time more than twice as fast as previous shimadzu systems, and before the next sample injection. Overview a fully functional tocl can be used for a variety of applications, such as quality control, process control, and.
The system should be toctn for internal sparging and toctn2 for external sparging. Examining the role of toc analyzers in the pharmaceutical. A collect sample in burned, amber glass bottle with teflon lid. Shimadzu 680 c combustion catalytic oxidation ndir detection method measurement system combining experience and reliability features the most important feature of a toc analyzer is its ability to efficiently oxidize not only easily decomposed, low molecular weight organic compounds, but also hardtodecompose insoluble and macromolecular organic compounds. How do you prepare soil samples to measure total organic carbon for shimadzu tocv csn. A nonspecific technique identifies the presence of all the chemicals in the analyzed sample, i. Combustion catalytic oxidationndir method combustion catalytic oxidationndir method tocvcs basic model, incorporating all essential functions.